X-ray Magnetic Circular Dichroism (XMCD) beamline

Beamline overview

X-ray Magnetic Circular Dichroism (XMCD) spectroscopy is used to determine element specific magnetic properties of materials as well as individual contributions of orbital and spin magnetic moments into total magnetic moment. The technique uses circularly polarized light of opposite helicity provided by the APPLE-II type helical undulator at XMCD beamline, BL-20. The beamline covers energy range from 300 -1000 eV for circular polarization and 300-2000 eV for plane polarization by using Varied Line Spacing Plane Gratings (VLS-PG) in Monk-Gillieson configuration. The monochromator can be operated in constant included angle mode as well as variable included angle mode. The monochromatized beam is focused by a toroidal mirror to a spot of ~ 400 µm (H) × 100 µm (V) at the sample. The experimental station of BL-20 is a UHV chamber with electromagnets placed outside. The typical pole gap inside the chamber is ~ 20 mm. There is a hole of ~ 13 mm diameter at the centre of pole of the electromagnets from where x-ray beam enters in the experimental station. It is equipped with a cryogen free cryostat to vary sample temperature in the range of 20 to 325 K.

The Beamline

Beamline parameters & Optical layout

The XMCD beamline (BL-20) uses circularly and plane polarized light emitted by an APPLE-II type helical undulator, U3.

Source parameters
Undulator typeAPPLE-II type helical undulator (U3)
Periodic Length56 mm
Number of Periods30
Peak Magnetic Field0.86 Tesla
Circular polarization modeBx = By0.29 Tesla
Kx = Ky1.5
Plane polarization modeBx, By0.325 Tesla, 0.535 Tesla
Kx, Ky1.7, 2.8
Beamline parameters & Optical layout
Beamline Parameters
Energy Range300 eV to 1000 eV in circular polarization mode
300 eV to 2000 eV in plane polarization mode
Resolution (calculated)30 meV at 300 eV of photon energy
Flux (calculated)1.5×1011photons/sec/200 mA at 300 eV of photon energy
Beam Size400 µm (H) × 100 µm (V)
MonochromatorTwo VLS-Plane Gratings


Optical layout of the XMCD beamline
Optical layout of the XMCD beamline
  1. First optical element is a vertically mounted toroidal mirror, TM1, which deflects the incoming beam horizontally at an angle of 3.5o (grazing angle of incident is 1.75o). It focuses the beam from the undulator vertically on to the entrance slit.
  2. The monochromator of the beamline consists of a spherical mirror (SM), one long plane mirror (PM) and two VLS-Plane Gratings (900 lines/mm and 1800 lines/mm). The monochromator is designed in such a way that it can be used in both Variable Included Angle (VIA) mode and in Constant Included Angle (CIA) mode.
  3. The post focusing optical elements are two horizontally mounted toroidal mirrors, M1, and M2, which focuses the beam on the samples into two experimental chambers. At present, we have only toroidal mirror (M1) and one experimental station (Expt-1). The other toroidal mirror (M2) and experimental station (Expt-2) are planned for future.

Experimental station

The experimental station of BL-20 is a UHV chamber with electromagnets placed outside. The typical pole gap inside the chamber is 20 mm. There a hole of ~ 13 mm diameter at the center of pole of the electromagnets from where the x-ray beam enters in the experimental station. It is equipped with a cryogen free cryostat to vary sample temperature in the range of 20 to 325 K.

Experimental Station Parameters
MagnetElectromagnet
Pole gap20 mm
Magnetic field at sample0 to 1 Tesla
Accessible sample space15 mm
Sample temperature20 to 325 K
Mode of measurementTotal electron yield (TEY)
Experimental station

Application Areas

Applied research Element specific magnetic properties of materials (bulk and thin films).

Individual contributions of orbital and spin magnetic moments in total magnetic moment.
ChemistryBonding arrangement of a particular atom in a compound using x-ray absorption near edge spectroscopy.
Phase transitionTemperature dependent measurements to determine the magnetic properties across the crystallographic or magnetic phase transitions.
Basic researchDetermination of unoccupied partial density of states, polarization based x-ray absorption of novel materials.


Science Highlights

Science Highlights
Effect of electronic transitions on near edge optical properties of off-stoichiometric boron carbide thin films

J. Appl. Phys. 133, 165302 (2023). https://doi.org/10.1063/5.0145828


Science Highlights
Assessment of bonding character of β-(AlxGa1-x)2O3 alloys from photoluminescence and x-ray absorption near edge spectroscopy

Appl. Phys. Lett. 122, 152104 (2023). https://doi.org/10.1063/5.0148800


Science Highlights
Boron migration during amorphous to crystalline transformation in CoFeB/MgO multilayers: A reflectivity study

Materials Research Bulletin 161, 112150, (2023) https://doi.org/10.1016/j.materresbull.2023.112150


Science Highlights
Interface analysis of Mg/Sc and Sc/Mg bilayers using X-ray reflectivity

Thin Solid Films 763, 139595 (2022). https://doi.org//10.1016/j.tsf.2022.139595


Science Highlights
J. Synchrotron Rad. 29 (2022) https://doi.org/10.1107/S1600577522004738


Science Highlights
J. Phys. D: Appl. Phys. 55, 185304 (2022) https://doi.org/10.1088/1361-6463/ac43dc


Science Highlights
Thin Solid Films 721 (2021) 138552 https://doi.org/10.1016/j.tsf.2021.138552


Science Highlights
J. Synchrotron Rad. 28 (2021) 224–230 https://doi.org/10.1107/S1600577520013429


Science Highlights
Applied Optics 60 (2021) 89 https://doi.org/10.1364/AO.400508

Team members

  1. Dr. Tapas Ganguli
  2. Dr. Shreyashkar Dev Singh
  3. Dr. Ravindra Jangir
  4. Shri Sudip Kumar Nath
  5. Shri Kiran Baraik
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